[1] HUIE CW.A review of modern sample-preparation techniques for the extraction and analysis of medicinal plants[J]. Anal Bioanal Chem,2002,373(1):23
[2] DENG C,LIU N,GAO M,et al.Recent developments in sample preparation techniques for chromatography analysis of traditional Chinese medicines[J]. J Chromatogr A,2007,1153(1):90
[3] TANG F,ZHANG Q,NIE Z,et al.Sample preparation for analyzing traditional Chinese medicines[J]. Trac Trend Anal Chem,2009,28(11):1253
[4] XIA L,LI Y,LIU Y,et al.Recent advances in sample preparation techniques in China[J]. J Sep Sci,2019,43:189
[5] JIN W,ZHOU T,LI G.Recent advances of modern sample preparation techniques for traditional Chinese medicines[J]. J Chromatogr A,2019,1606:460377
[6] GROSSO C,COELHO JP,PESSOA FLP,et al.Mathematical modelling of supercritical CO2 extraction of volatile oils from aromatic plants[J]. Chem Eng Sci,2010,65(11):3579
[7] MANJARE SD,DHINGRA K.Supercritical fluids in separation and purification:a review[J]. Mater Sci for Energy Tech,2019,2(3): 463
[8] SOLANA M,BOSCHIERO I,DALL'ACQUA S,et al.A comparison between supercritical fluid and pressurized liquid extraction methods for obtaining phenolic compounds from Asparagus officinalis L.[J]. J Supercrit Fluids,2015,100:201
[9] HE JZ,SHAO P,LIU JH,et al.Supercritical carbon dioxide extraction of flavonoids from Pomelo(Citrus grandis (L.) Osbeck) peel and their antioxidant activity[J]. Int J Mol Sci,2012,13(10): 13065
[10] RUAN X,YAN LY,LI XX,et al.Optimization of process parameters of extraction of amentoflavone,quercetin and ginkgetin from taxus chinensis using supercritical CO2 Plus Co-Solvent.[J]. Molecules, 2014,19:17682
[11] GHAFOOR K,AL-JUHAIMI FY,CHOI YH.Supercritical fluid extraction of phenolic compounds and antioxidants from grape(vitis labrusca B.) seeds[J]. Plant Food Hum Nutr,2012,67(4):407
[12] NUMAN-AL-MOBIN AM,KOLLA P,DIXON D,et al.Effect of water-carbon dioxide ratio on the selectivity of phenolic compounds produced from alkali lignin in sub-and supercritical fluid mixtures[J]. Fuel,2016,185:26
[13] MARTINS PF,DE MELO MMR,SARMENTO P,et al.Supercritical fluid extraction of sterols from Eichhornia crassipes biomass using pure and modified carbon dioxide.Enhancement of stigmasterol yield and extract concentration[J]. J Supercrit Fluids,2016,107:441
[14] 崔勇,李青,刘思洁,等.固相萃取-超高效液相色谱法同时测定人参中11 种人参皂苷的含量[J]. 中国卫生检验杂志,2012, 22:475
CUI Y,LI Q,LIU SJ,et al.Simultaneous determination of content of 11 kinds of ginsenoside in ginseng by ultra performance liquid chromatography[J]. Chin J Health Lab Techhd,2012,22(3):475
[15] 朱定姬,卢敏萍,黄克建,等.在线固相萃取结合液相色谱-线性离子阱多级质谱法同时检测生物样品中7 种乌头类生物碱[J]. 色谱,2016,34(3):249
ZHU DJ,LU MP,HUANG KJ,et al.Simultaneous determination of seven aconitum alkaloids in biological samples by liquid chromatography-linear ion trap multistage mass spectrometry coupled with on-line solid phase extraction[J]. Chin J Chrom,2016,34(3): 249
[16] 蒋银燕,郭丽娟,崔小莹,等.活性炭固相萃取/胶束电动色谱联用技术用于雷公藤3 种有效成分的测定[J]. 分析测试学报, 2015,34(2):189
JIANG YY,GUO LJ,CUI XY,et al.Determination of three active components in Tripterygium wilfordii Hook. f.by activated carbon solid phase extraction combined with micellar electro kinetic capillary chromatography[J]. J Inst Anal,2015,34(2):189
[17] 孙健,李丽敏,胡青,等.注射用银杏叶提取物及其制剂中总银杏酸含量的测定[J]. 世界中医药,2019,14(4):818
SUN J,LI LM,HU Q,et al.Determination of total ginkgolic acid in Ginkgo biloba extract and its preparation for injection[J]. World J Tradit Chin Med,2019,14(4):818
[18] 侯建波,谢文,钱艳,等.固相萃取-液相色谱-串联质谱法同时测定蜂蜜中16 种黄酮类化合物和阿魏酸[J]. 色谱,2020,38(5):529
HOU JB,XIE W,QIAN Y,et al.Simultaneous determination of 16 flavonoids and ferulic acid in honey by solid phase extraction-liquid chromatography-tandem mass spectrometry[J]. Chin J Chromatogr, 2020,38(5):529
[19] 吕辰,丁涛,马昕,等.高效液相色谱-串联质谱法测定蜂蜜中的5 种双稠吡咯啶类生物碱[J]. 色谱,2013,31(11):1046
Lü C,DING T,MA X,et al.Determination of five pyrrolizidine alkaloids in honey by liquid chromatography-tandem mass spectrometry[J]. Chin J Chromatogr,2013,31(11):1046
[20] 史煜华,黄文康,黄琴伟,等.SPE-HPLC 测定风湿骨痛片中6 种生物碱类物质的含量[J]. 中国现代应用药学,2018,35(12): 47
SHI YH,HUANG WK,HUANG QW,et al.Content determination of six Alkaloids in Fengshigutong tablet by SPE-HPLC[J]. Chin J Mod Appl Pharm,2018,35(12):47
[21] 梁晟,杨青,李瑞莲,等.UPLC-MS/MS 法测定13 种中成药中的马兜铃酸A[J]. 华西药学杂志,2020,35(1):78
LIANG S,YANG Q,LI RL,et al.Determination of aristolochic acid A in 13 kinds of traditional Chinese patent medicines by UPLC-MS/MS[J]. West China J Pharm Sci,2020,35(1):78
[22] 舒翔,陈军,林世和,等.大黄清胃丸中马兜铃酸A 的限量检测[J]. 中国医院药学杂志,2016,36(17):1512
SHU X,CHEN J,LIN SH,et al.Determination of limit of aristolochic acid A in Dahuang Qingwei Wan[J]. Chin J Hosp Pharm,2016,36(17):1512
[23] 张莉,陈飞,红玉,等.固相萃取-手性气相色谱法测定醒脑静注射液中右旋龙脑和麝香酮的含量[J]. 海峡药学,2017,29(4): 68
ZHANG L,CHEN F,HONG Y,et al.Simultaneous determination of D-borneol and muscone in Xingnaojing injection by SPE and chiral capillary gas chromatography[J]. Strait Pharm J,2017,29(4):68
[24] 谢辉,陈亚,雷爱玲,等.SPE-HPLC-DAD 法同时检测柑橘药用资源中黄烷酮类和川陈皮素成分[J]. 天然产物研究与开发, 2019,31(8):1365
XIE H,CHEN Y,LEI AL,et al.Simultaneous determination of flavanones and nobiletin in citrus medicinal resources by using SPE-HPLC-DAD methods[J]. Nat Prod Res Dev,2019,31(8):1365
[25] 缪菊连,黄照昌,王成军,等.HPLC-ELSD 法测定生脉饮中麦冬皂苷 D[J]. 中成药,2015,37(2):462
MIAO JL,HUANG ZC,WANG CJ,et al.Determination of ophioposide D in Shengmaiyin by HPLC-ELSD[J]. Chin Tradit Pat Med,2015,37(2):462
[26] 李效宽,张艳海,冯天辉,等.在线固相萃取法结合电雾式检测器测定黄芪及其复方中黄芪甲苷的含量[J]. 分析化学,2014, 42(12):1791
LI XK,ZHANG YH,FENG TH,et al.Determination of atragaloside IV in Radix Astragli and its preparations by online SPE-liquid chromatography with charged aerosol detector[J]. Chin J Anal Chem,2014,42(12):1791
[27] 齐广才,吴江瑞,崔生飞,等.固相萃取-高效液相色谱法测定泻痢固肠片中芍药苷、甘草苷、橙皮苷的含量[J]. 中南药学, 2016,14(4):418
QI GC,WU JR,CUI SF,et al.Determination of paeoniflorin, liquiritin and hesperidin in Xieli Guchang tablets by SPE-HPLC[J]. Centr South Pharm,2016,14(04):418
[28] 赵娜娜,刘汇,孙道磊,等.血塞通中皂苷类成分的SPE-ESI-MS/MS分析[J]. 吉林中医药,2018,38(3):328
ZHAO NN,LIU H,SUN DL,et al.SPE-ESI-MS/MS analysis of ginsenosides in Xuesaitong[J]. Jilin J Tradit Chin Med,2018,38(3):328
[29] 王绍弛. “食药两用”菊花中多农药残留分析方法建立及应用[D]. 哈尔滨:东北农业大学,2019
WANG SC.Development and Application of Multi-Pesticides Residue Analytical Method in Complex Chrysanthemum Samples[D]. Haerbin:Northeast Agricultural University,2019
[30] 郝经文,徐文冬,石敏珠,等.GC-MS 同时测定霍山石斛及霍山产铁皮石斛中拟除虫菊酯和氨基甲酸酯类16 种农药残留的检测方法[J]. 食品工业科技,2019,40(9):230
HAO JW,XU WD,SHI MZ,et al.Simultaneous determination of 16 kinds of pyrethroid and carbamate pesticide residues in Dendrobium huoshanense and Dendrobium officinale from Huoshan by GC-MS[J]. Sci Tech Food Ind,2019,40(9):230
[31] 黄绍军,李超,马成章,等.气相色谱-串联质谱法测定玉龙县人参中农药残留量[J]. 分析试验室,2017,36(4):423
HANG SJ,LI C,MA CZ,et al.Simultaneous determination of pesticide residues in Yulong County ginseng by gas chromatography-tandem mass spectrometry[J]. Chin J Anal Lab,2017,36(4):423
[32] 郑培,冯春艳,赵晓野.UPLC-MS/MS 法同时测定裸花紫珠药材中 9 种农药残留[J]. 海南医学,2018,29(16):2309
ZHENG P,FENG CY,ZHAO XY.Simultaneous determination of 9 pesticide residues in medicinal Callicarpa nudiflora by UPLC-MS/MS[J]. Hainan Med J,2018,29(16):2309
[33] 林祥群,卢春霞,罗小玲,等.气相色谱-质谱法测定枸杞中28 种农药残留[J]. 江苏农业科学,2016,44(1):285
LIN XQ,LU CX,LUO XL,et al.Simultaneous determination of 28 pesticides residues in Chinese wolfberry(Lycium chinense L.) by gas chromatography-mass spectrometry[J]. Jiangsu Agric Sci, 2016,44(1):285
[34] 吴娜,刘卫,严和平,等.中药材三七中农药多残留分析的样品前处理方法[J]. 药学学报,2013,48(10):1585
WU N,LIU W,YAN HP,et al.Sample pretreatment methods of pesticide residues in Panax notoginseng of Chinese traditional medicine[J]. Acta Pharm Sin,2013,48(10):1585
[35] 刘桂宁,强维,钟闱桢,等.固相萃取/毛细管气相色谱法测定肉桂皮中六六六、滴滴涕农药残留量[J]. 分析测试学报,2014, 33(1):103
LIU GN,QING W,ZHONG WZ,et al.Determination of BHC and DDT pesticide residues in Cinnamomum cassia bark by solid-phase extraction and capillary gas chromatography[J]. J Inst Anal,2014, 33(1):103
[36] 李继革,施家威,王玉飞.固相萃取-气相色谱-串联质谱法测定绞股蓝中75 种农药残留[J]. 中国卫生检验杂志,2017, 27(19):2746
LI JG,SHI JW,WANG YF.Determination of 75 pesticides in Gynostemma pentaphylla using solid-phase extraction and gas chromatography-tandem mass spectrometry[J]. Chin J Heal Lab Tech,2017,27(19):2746
[37] 祁伟,豆小文,付延伟,等.固相萃取-气相色谱-串联质谱法快速监测酸枣仁中有机氯类农药残留[J]. 食品安全质量检测学报,2019,10(10):2929
QIW,DOU XW,F U YW,et al.Rapid determinatin of organochlorine pesticide in Ziziphi Spinosae Semen by Carb/NH2-solid phase extraction-gas chromatography-tandem mass spectrometry[J] J.Food Saf Qual,2019,10(10):2929
[38] 张园,张琦,王贤亲.固相萃取-气相色谱串联质谱法测定温莪术中19 种有机氯和有机磷农药残留[J]. 药物分析杂志,2012, 32(1):95
ZHANG Y,ZHANG Q,WANG XQ.SPE-GC/MS determination of 19 organophosphorus pesticide residues and organochlorine pesticide residues in Rhizoma Curcumae[J]. Chin J Pharm Anal,2012,32(1):95
[39] 张海燕. 固相萃取-气相色谱法测定甘草中的六六六、滴滴涕含量[J]. 化学分析计量,2015,24(5):52
ZHANG HY.Determination of BHC and DDT pesticide residues in licorice by solid-phase extraction and capillary gas chromatography[J]. Chem Anal Mete,2015,24(5):52
[40] 秦伟瀚,阳勇,师萱,等.基质分散固相萃取法同时检测13 种不同产地昆明山海棠中有机磷和拟除虫菊酯类农药残留[J]. 中国医院药学杂志,2017,37(7):613
QIN WH,YANG Y,SHI X,et al.Simultaneous determination of organophosphorus pesticide and pyrethroid pesticide residues from 13 different habitats of Tripterygium hypoglaucum(Levl.) Hutch by matrix solid phase extraction[J]. Chin J Hosp Pharm,2017,37(7): 613
[41] 粟有志,刘俊,李艳美,等.固相萃取-高效液相色谱-串联质谱法测定枸杞中9 种红色合成色素[J]. 分析科学学报,2016, 32(6):846
SU YZ,LIU J,LI YM,et al.Determination of 9 red synthetic pigments in Chinese wolfberry by solid-phase extraction-high performance liquid chromatography-tandem mass spectrometry[J]. J Anal Sci,2016,32(6):846
[42] 余诗琪,汪波,吕盼,等.固相萃取-液质联用法测定土鳖虫中12 种真菌毒素[J]. 世界科学技术-中医药现代化,2019,21(7):1411
YU SQ,WANG B,Lü P,et al.Determination of 12 mycotoxins in Eupolyphaga Seu Steleophaga by solid-phase extraction coupled with high performance liquid chromatography-tandem mass spectrometry[J]. World Sci Technol-Mod Tradit Chin Med,2019,21(7):1411
[43] 李拓,叶小敏,聂小春.固相萃取-电喷雾高效离子迁移谱法快速检测红花中4 种非法添加染色物质[J]. 中国药师,2017,20(8):1349
LI T,YE XM,NIE XC.Rapid determination of four illegally added staining substances in safflower by solid phase extraction-electrospray ionization-high performance ion mobility spectrometry[J]. China Pharm,2017,20(8):1349
[44] 姜伟,张璐,傅小红,等.阴离子交换固相萃取-HPLC 快速测定中药材中合成色素的方法研究[J]. 北方药学,2016,13(10):2
JIANG W,ZHANG L,FU XH,et al.Rapid determination of synthetic pigments in medicinal Chinese herbs by anion exchange SPE-HPLC[J]. J North Pharm,2016,13(10):2
[45] TURIEL E,MARTÍN-ESTEBAN A.Molecularly imprinted polymers for sample preparation:a review[J]. Anal Chim Acta,2010, 668(2):87
[46] NCUBE S,MADIKIZELA LM,NINDI MM,et al.Solid Phase Extraction Technique As A General Field Of Application Of Molecularly Imprinted Polymer Materials[M]. Amsterdam: Elsevier,2019:41
[47] PARDO A,MESPOUILLE L,DUBOIS P,et al.Targeted extraction of active compounds from natural products by molecularly imprinted polymers[J]. Cent Eur J Chem,2012,10(3):751
[48] ZHAI C,LU Q,CHEN X,et al.Molecularly imprinted layer-coated silica nanoparticles toward highly selective separation of active diosgenin from Dioscorea nipponica Makino[J]. J Chromatogr A, 2009,1216(12):2254
[49] LUO J,ZHANG L,CHEN D,et al.Molecularly imprinted layer-coated monodisperse spherical silica microparticles toward affinity-enrichment of isoflavonoid glycosides from Radix Puerariae[J]. Analyst,2012,137(12):2891
[50] EIDI S,IRANSHAHI M,MOHAMMADINEJAD A,et al.Selective isolation of sesquiterpene coumarins from asafoetida using dummy molecularly imprinted solid phase extraction method[J]. J Chromatogr B,2020,1138:121943
[51] MACHYŇÁ oil[J]. Anal Chim Acta,2012,734:99
[62] LI X,WANG Y,SUN Q,et al.Molecularly imprinted solid phase extraction in a syringe filter for determination of triazine herbicides in Radix Paeoniae Alba by ultra-fast liquid chromatography[J]. Talanta,2016,148:539
[63] XU X,LIANG S,MENG X,et al.A molecularly imprinted polymer for the selective solid-phase extraction of dimethomorph from ginseng samples[J]. J Chromatogr B,2015,988:182
[64] 李亚丽,朴向民,曲正义,等.磁性固相萃取技术在食品和中药材分析前处理中的应用进展[J]. 食品安全质量检测学报,2020, 11(2):443
LI YL,PAO XM,QU ZY,et al.Advance in the application of magnetic solid-phase extraction in pre-treatment of foods and traditional Chinese medicinal materials[J]. J Food Saf Qual,2020, 11(02):443
[65] 殷召军. 磁性固相萃取技术在测定大黄蒽醌类成分中的应用[J]. 中国现代中药,2018,20(7):860
YIN ZJ.Application of magnetic solid-phase extraction technology in determination of anthraquinones constituents in Rheum palmatum[J]. Mod Chin Med,2018,20(7):860
[66] 义西求吉,周加本,热增才旦,等.MSPE-HPLC 法测定甘青青兰中5 种黄酮化合物含量[J]. 分析试验室,2020,39(4):379
YIXI QJ,ZHOU JB,REZENG CD,et al.Simultaneous determination of five flavonoids in Dracocephalum tanguticum with MSPE-HPLC[J]. Chin J Anal Labor,2020,39(4):379
[67] 李清,楚楚,魏蒙蒙,等.功能化磁性纳米颗粒用于生脉饮(党参方)中黄曲霉毒素B1 的含量测定[J]. 药物分析杂志,2017,37(10):1890
LI Q,CHU C,WEI MM,et al.Application of functional magnetic nanoparticles in determination of aflatoxin B1 in Shengmai decoction (Dangshen prescription)[J]. Chin J Pharm Anal,2017,37(10): 1890
[68] ZHANG HF,SHI YP.Pretreatment properties of CTAB coated Fe3O4 nanoparticle mixed hemimicelle sorbents for the analysis of herbal medicine samples[J]. Cur Anal Chem,2012,8(1):150
[69] ZHANG HF,SHI YP.Magnetic retrieval of chitosan:extraction of bioactive constituents from green tea beverage samples[J]. Analyst, 2012,137
[70] HERRERO LATORRE C,ÁLVAREZ MÉNDEZ J,BARCIELA GARCÍA J,et al.Carbon nanotubes as solid-phase extraction sorbents prior to atomic spectrometric determination of metal species: a review[J]. Anal Chim Acta,2012,749:16
[71] LI N,JIANG HL,WANG X,et al.Recent advances in graphene-based magnetic composites for magnetic solid-phase extraction[J]. TrAC Trends Anal Chem,2018,102:60
[72] BARKER SA.Matrix solid phase dispersion (MSPD J]. J Biochem Biophgs Meth,2007,70(2):151
[73] ŚMIEŁOWSKA M,ZABIEGAŁA B.Matrix solid-phase dispersion (MSPD) as simple and useful sample preparation technique for
determination of polybrominated diphenyl ethers (PBDEs) in dust[J]. Anal Chim Acta,2019,1084:33
[74] CAPRIOTTI A L,CAVALIERE C,GIANSANTI P,et al.Recent developments in matrix solid-phase dispersion extraction[J]. J Chromatogr A,2010,1217(16):2521
[75] CAPRIOTTI AL,Cavaliere C,Laganà A,et al.Recent trends in matrix solid-phase dispersion[J]. TrAC Trends Anal Chem,2013, 43:53
[76] CAPRIOTTI AL,CAVALIERE C,FOGLIA P,et al.Recent advances and developments in matrix solid-phase dispersion[J]. TrAC Trends Anal Chem,2015,71:186
[77] SHI X,LI X,LIU J,et al.Lignan extraction from the roots of Sinopodophyllum emodi Wall by matrix solid-phase dispersion[J]. Chromatographia,72(7-8):713
[78] JIN YR,SHI XL,LI XW,et al.Matrix Solid Phase Dispersion for the Extraction of Podophyllotoxin Glucoside and isopicropodophyllone from roots of Sinopodophyllum emodi (Wall.)[J]. Chem J Chin UUV,2011,32(5):1054
[79] DONG X,YANG J,ZHENG XI,et al.Ion pair assisted micro matrix solid phase dispersion extraction of alkaloids from medical plant[J]. Electrophoresis,2019,41(1-2):123
[80] WEI W,LI XW LI,SHI XL,et al.Matrix solid-phase dispersion extraction of alkaloids from the roots of Aconitum kusnezoffii Reichb[J]. Chem Res Chin U,2011,027(001):23
[81] DU L J,HUANG J P,WANG B,et al.Carbon molecular sieve based micro-matrix-solid-phase dispersion for the extraction of polyphenols in pomegranate peel by UHPLC-Q-TOF/MS[J]. Electrophoresis,2018,39(17):2218
[82] HONG B,WANG Z,XU T,et al.Matrix solid-phase dispersion extraction followed by high performance liquid chromatography-diode array detection and ultra performance liquid chromatography-quadrupole-time of flight-mass spectrometer method for the determination of the main compounds from Carthamus tinctorius L. (Hong-hua)[J]. J Pharm Biom Anal,2015,107:464
[83] DU KZ,LI J,GAO XM,et al.Ultrasound-enhanced matrix solid-phase dispersion micro-extraction applying Mesoporous Molecular Sieve SBA-15 for the determination of multiple compounds in Fructus Psoraleae[J]. Sustain Chem Pharm,2020,15:100198
[84] GE L,YONG JWH,TAN SN,et al.Simultaneous extraction, separation,isolation and identification of endogenous components from Etlingera elatior by pressurized matrix solid-phase dispersion using liquid chromatography-mass spectrometry[J]. J Chromatogr A,2020,1611:460604
[85] CHEN SJ,DU KZ,LI J,et al.A chitosan solution-based vortex-forced matrix solid phase dispersion method for the extraction and determination of four bioactive constituents from Ligustri Lucidi Fructus by high performance liquid chromatography[J]. J Chromatogr A,2020,1609:460509
[86] 杨璐,代琳男,李丽,等.基质分散固相萃取-高效液相色谱法测定板蓝根中药饮片中多菌灵的残留量[J]. 海峡药学,2013, 25(9):65
YANG L,DAI LN,LI L,et al.Determination of carbendazim residue in Chinese decoction pieces of Isatis roots by dispersive solid phase extraction-HPLC[J]. Strait Pharm J,2013,25(9):65
[87] 秦伟瀚,阳勇,师萱,等.基质分散固相萃取法同时检测13 种不同产地昆明山海棠中有机磷和拟除虫菊酯类农药残留[J]. 重庆中草药研究,2017,37(7):613
QIN WH,YANG Y,SHI X,et al.Simultaneous determination of organophosphorus pesticide and pyrethroid pesticide residues from 13 different habitats of Tripterygium hypoglaucum (Levl.) Hutch by matrix solid phase extraction[J]. Chongqing Chin J Hos Pharm, 2017,37(7):613
[88] 陈一鑫,冯清胜,王晓中,等.离子液体-基质固相分散-超声雾化-固相萃取结合高效液相色谱法检测人参中三嗪类除草剂[J]. 分析化学,2016,44(7):1106
CHEN YX,FENG QS,WANG XZ,et al.Determination of trzaine Herbicides in Panax ginseng C.A.mey by silica supported ionic liquid-matrix solid phase dispersion-ultrasonic-assisted nebulization extraction-solid phase extraction followed by high-performance liquid chromatography[J]. Chin J Anal Chem,2016,44(07): 1106
[89] QI X.Development of a matrix solid-phase dispersion-sonication extraction method for the determination of fungicides residues in ginseng extract[J]. Food Chem,2010,121(3):758
[90] 马微,程丽,张兰威,等.基质分散固相萃取-高效液相色谱-串联质谱法同时测定减肥保健食品中20 种违禁添加药物[J]. 分析化学,2014,42(8):1161
MA W,CHENG L,ZHANG LW,et al.Simultaneous determination of 20 anti-obesity drugs illegally added in weight-loss functional foods by matrix solid phase dispersion-high perform liquid chromatography tandem mass spectrometry[J]. Chin J Anal Chem, 2014,42(8):1161
[91] ANASTASSIADES M,MASTOVSKÁ K,LEHOTAY SJ.Evaluation of analyte protectants to improve gas chromatographic analysis of pesticides[J]. J Chromatogr A,2003,1015(1-2):163
[92] COSTA FP,CALDAS SS,PRIMEL EG.Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in canned and fresh peach[J]. Food Chem,165:587
[93] 刘琪. 改进QuEChERS 技术结合GC-MS/MS 测定西洋参中的农药多残留[D]. 济南:山东农业大学,2019
LIU Q.Improved QuEChERS Technology Combined with GC-MS/MS to Determine Pesticide Residues in American Ginseng[D]. Jinan:Shandong Agriculture University,2019
[94] 李雯婷,苗水,陈铭,等.液相色谱-串联质谱法同时测定丹参中139 种农药残留[J]. 世界中医药,2019,14(4):783
LI WT,MIAO S,CHEN M,et al.Simultaneous determination of 139 pesticide residues in Salvia miltiorrhiza by LC-MS/MS[J]. World Chin Med,2019,14(4):783
[95] 王明辉. 改进QuEChERS 技术结合色谱–串联质谱分析金银花和菊花中的农药多残留[D]. 济南:山东农业大学,2019
WANG MH.Improved QuEChERS Technology Combined with GC-MS/MS to Determine Pesticide Residues in Honeysuckle and Chrysanthemum[D]. Jinan:Shandong Agriculture University,2019
[96] 马桂娟,朱捷,汤丽华,等.分散固相萃取-UPLC-MS/MS 同时测定枸杞籽油中14 种真菌毒素[J]. 食品与发酵科技,2019, 55(1):95
MA GJ,ZHU J,TANG LH,et al.Determination of 14 mycotoxins in lycium seed oil by dispersive solid-phase extraction combined with ultra high performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS)[J]. Sic Food Ferment,2019,55(1):95
[97] CHEN L,JIA X,LU Q,et al.Highly efficient and selective enrichment of puerarin from Radix Puerariae by molecularly imprinted solid-phase extraction[J]. sep Purif Technol,2010,71(3):324
[98] FU Q,FANG Q,FENG B,et al.Matrine-imprinted monolithic stationary phase for extraction and purification of matrine from Sophorae flavescentis Ait.[J]. J Chromatogr B,879(13-14):894
[99] ZHU H,WANG Y,YUAN Y,et al.Development and characterization of molecularly imprinted polymer microspheres for the selective detection of kaempferol in traditional Chinese medicines[J]. Anal Methods,2011,3(2):348
[100] LIN PYW,HUAN Z,YUAN Y.Molecularly imprinted polymer for solid-phase extraction of rutin in complicated traditional Chinese medicines[J]. Analyst,2011,136(4):756
[101] YIN X,LIU Q,JIANG Y,et al.Development of andrographolide molecularly imprinted polymer for solid-phase extraction[J], Spectrochim Acta,2011,79(1):191
[102] VUSUMZI P,EWA C,SOFIA L,et al.Molecular imprinted polymer for solid-phase extraction of flavonol aglycones from Moringa oleifera extracts[J]. J Sep Sci,2013,36(3):548
[103] HONG Y,CHEN L.Extraction of quercetin from Herba Lysimachiae by molecularly imprinted-matrix solid phase dispersion[J]. J Chromatogra B,2013,941:38
[104] MOHAJERI SEYED A,HOSSEINZADEH H,KEYHANFAR F,et al.Extraction of crocin from saffron(Crocus sativus) using molecularly imprinted polymer solid-phase extraction[J]. Clin Biochem,2011,44(13 Suppl):S136
[105] YUAN Y,WANG Y,HUANG M,et al.Developmentand characterization of molecularly imprinted polymers for the selective enrichment of podophyllotoxin from traditional Chinese medicines[J]. Anal Chim Acta,2011,695(1-2):63
[106] HROBOŇOVÁ K,MACHYŇÁKOVÁ A,ČIŽMÁRIK J. Determination of dicoumarol in Melilotus officinalis L .by using molecularly imprinted polymer solid-phase extraction coupled with high performance liquid chromatography[J]. J Chromatogr A, 2018,1539:93
[107] CHEN L,JI W,DUAN W,et al.Effectively designed molecularly imprinted polymers for selective extraction of glabridin from Glycyrrhiza glabra L .residues by screening the library of non-imprinted polymers[J]. J Chromatogr B,2014,965:1
[108] YU H,HE Y,SHE Y,et al.Preparation of molecularly imprinted polymers coupled with high-performance liquid chromatography for the selective extraction of salidroside from Rhodiola crenulata[J]. J Chromatogra B,2019,1118-1119:180
[109] ATLABACHEW M,TORTO N,CHANDRAVANSHI BS.Matrix Solid-Phase Dispersion for the HPLC-DAD determination of psychoactive phenylpropylamino Alkaloids from khat(Catha edulis Forsk) chewing leaves[J]. Chromatographia,2013,76(7-8): 401
[110] BARDIA M,BAHRAM D,PEYMAN H,et al.Matrix solid phase dispersion extraction for Tropane alkaloid detection in cultured and collected Hyoscyamus reticulatus plants[J]. Int J Adv Res,2015, 3(11):78
[111] ANNA O,KRYSTYNA SW,TOMASZ O,et al.Matrix solid-phase dispersion versus ultrasound assisted extraction with solid-phase extraction in the HPLC analysis of furanocoumarins from fruits of archangelica officinalis Hoffm.[J]. J Braz Chem Soc,2014, 25(7):1166
[112] ONISZCZUK A,WAKSMUNDZKA-HAJNOS M,SKALICKA-WOŹNIAK K,et al.Comparison of matrix-solid phase dispersion and liquid-solid extraction connected with solid-phase extraction in the quantification of selected furanocoumarins from fruits of Heracleum leskowii by high performance liquid chromatography[J]. Ind Crop Prod,2013,50:131
[113] CHEN C,FU Z,ZHOU W,et al.Ionic liquid-immobilized NaY zeolite-based matrix solid phase dispersion for the extraction of active constituents in Rheum palmatum L.[J]. Microchem J,2020,152: 104245
[114] HU YH,WANG QY,YE LH,et al.Effervescent salt and crown ether-assisted matrix solid-phase dispersion extraction of coumarins from Cortex fraxini[J]. Ind Crop Prod,2019,141:111752
[115] ZHANG Q,CAI D,LIU J.Matrix solid-phase dispersion extraction coupled with HPLC-diode array detection method for the analysis of sesquiterpene lactones in root of Saussurea lappa C.B.Clarke[J]. J Chromatogr B,2011,879(26):2809
[116] ZHANG Q,ZHU W,GUAN H,et al.Development of a matrix solid-phase dispersion extraction combined with high-performance liquid chromatography for determination of five lignans from the Schisandra chinensis[J]. J Chromatogr B,2016,1011:151
[117] CHU C,WEI M,WANG S,et al.Micro-matrix solid-phase dispersion coupled with MEEKC for quantitative analysis of lignans in Schisandrae Chinensis Fructus using molecular sieve TS-1 as a sorbent[J]. J Chromatogr B,2017,1063:174
[118] SHI X,JIN Y,LIU J,et al.Matrix solid phase dispersion extraction of ginsenosides in the leaves of Panax ginseng C.M.Mey[J]. Food Chem,2011,129(3):1253
[119] VISNEVSCHI-NECRASOV T,CUNHA SC,NUNES E,et al.Optimization of matrix solid-phase dispersion extraction method for the analysis of isoflavones in Trifolium pratense[J]. J Chromatogra A,2009,1216(18):3720
[120] WU W,QIAN W,HAO H,et al.Determination of caffeoylquinic acid derivatives in Azolla imbricata by chitosan-based matrix solid-phase dispersion coupled with HPLC-PDA[J]. J Pharm Biomed Anal,2019,163:197
[121] CAO J,PENG LQ,XU JJ.Microcrystalline cellulose based matrix solid phase dispersion microextration for isomeric triterpenoid acids in loquat leaves by ultrahigh-performance liquid chromatography and quadrupole time-of-flight mass spectrometry[J]. J Chromatogr A, 2016,1472:16
[122] 李漓,周小江,袁志鹰,等.分散固相萃取HPLC 测定玄参中五种指标性成分[J]. 海峡药学,2019,31(11):30
LI L,ZHOU XJ,YUAN ZY,et al.Determination of five index components in Scrophulariae by dispersive solid phase extraction[J]. Strait Pharm J,2019,31(11):30
[123] 许莉. 利用免疫亲和固相萃取检测小分子化合物的方法研究及其应用[D]. 北京:北京大学,2010
XU L.Contents Research and Application of Methods for Detecting Small Molecule Compounds Using Immunoaffinity Solid Phase Extraction[D]. Beijing:Peking University,2010
[124] 屈会化,赵琰,王庆国.中药小分子单克隆抗体技术平台的构建[J]. 中草药,2014,45(7):895-899
QU HH,ZHAO Y,WANG QG.Establishment of small molecular monoclonal antibody technology platform in Chinese materia medica[J]. Chin Tradit Herb Drugs,2014,45(7):895
[125] 屈保平,冯红,续洁琨,等.基于芍药苷单克隆抗体的ELISA 快速检测方法建立[J]. 药物分析杂志,2016,36(11):1931
QU BP,FENG H,XU JK,et al.Establishment of quick enzyme-linked immunosorbent assay with monoclonal antibody against paeoniflorin[J]. Chin J Pharm Anal,2016,36(11):1931
[126] 赵孔祥,胡筱芸,何佳,等.免疫亲和净化-液相色谱-串联质谱测定中成药中14 个真菌毒素[J]. 药物分析杂志,2012,32(5): 846
ZHAO KX,HU XY,HE J,et al.Determination of 14 mycotoxins in Chinese patent medicines by HPLC-MS/MS after immunoaffinity purification[J]. Chin J Pharm Anal,2012,32(5):846
[127] 韩深,刘萤,吕美玲,等.免疫亲和萃取-超高效液相色谱-串联质谱法分离测定中成药及中药材中的5 种黄曲霉毒素[J]. 色谱,2011,29(7):613
HAN S,LIU Y,Lü ML,et al.Determination of five aflatoxins in Chinese patent medicines and medicinal herbs by immunoaffinity extraction coupled with ultra-high performance liquid chromatography-tandem mass spectrometry[J]. Chin J Chromatogr,2011,29(7): 613
[128] XU CH,CHEN GS,XIONG ZH,et al.Applications of solid-phase
microextraction in food analysis[J]. J Chromatog A,2016,80(1-2):12
[129] HUANG B,LEI Y,TANG Y,et al.Comparison of HS-SPME with hydrodistillation and SFE for the analysis of the volatile compounds of Zisu and Baisu,two varietal species of Perilla frutescens of Chinese origin[J]. Food Chem,2011,125(1):268
[130] 韩蔓,江汉美,马银宇.HS-SPME-GC-MS 分析桑不同药用部位的挥发性成分[J]. 中国现代中药,2019,21(2):29
HAN M,JIANG HM,MA YY.Analysis of volatile components of different medicinal parts of Morus alba L.by HS-SPME-GC-MS[J]. Mod Chin Med,2019,21(2):29
[131] 郑海,周伟明,王如意,等.HS-SPME-GC-MS 法分析裸花紫珠不同部位挥发性成分[J]. 中成药,2018,40(7):1643
ZHENG H,ZHOU WM,WANG RY,et al.HS-SPME-GC-MS analysis of volatile components in different parts of nudeflower purple pearl[J]. Chin Trad Pat Med,2018,40(7):1643
[132] 韩蔓,江汉美,卢金清,等.HS-SPME-GC-MS 分析辛夷与其混用品的挥发性成分[J]. 湖北农业科学,2020,59(2):149
HAN M,JIANG HM,LU JQ,et al.Analysis of volatile components extracted from Magnoliae Flos and mixed product by HS-SPME-GC-MS[J]. Hubei Agric Sci,2020,59(2):149
[133] 刘梦菲,卢金清,江汉美,等.HS-SPME-GC-MS 分析益母草及其伪品夏至草的挥发性成分[J]. 中医药导报,2018,24(314):53
LIU MF,LU JQ,JIANG HM,et al.Analysis on the volatile components of Yimucao(Leonurus Japonicus Houtt.) and its counterfeit Xiazhicao (Lagopsis Supine) by HS-SPME-GC-MS[J]. Guiding J Tradit Chin Med Pharm,2018,24(314):53
[134] 梁欢,卢金清,戴艺,等.HS-SPME-GC-MS 结合化学计量法对不同产地艾叶药材挥发性成分的比较分析[J]. 中国实验方剂学杂志,2014,20(18):85
LIANG H,JU JQ,DAI Y,et al.Comparative analysis of volatile components of Artemisiae Argyi Folium from different origins using HS-SPME-GC-MS[J]. Chin J Exp Trad Med Form,2014, 20(18):85
[135] 卢金清,郭彧,李雨玲,等.HS-SPME-GC-MS 对不同产地南沙参挥发性化学成分的研究[J]. 湖北中医杂志,2013,35(3):71
LU JQ,GUO Y,LI YL,et al.HS-SPME-GC-MS Study on volatile chemical constituents of adenophora from different places[J]. Hubei J Trad Chin Med,2013,35(3):71
[136] 龚敏,卢金清,韩怡.HS-SPME-GC-MS 分析荆芥及其炮制品的挥发性成分[J]. 中国现代中药,2019,21(8):1041
GONG M,LU JQ,HAN Y.Analysis of volatile components of Schizonepeta tenuifolia and its processed products by HS-SPME-GC-MC[J]. Mod Chin Med,2019,21(8):1041
[137] 马银宇,卢金清,彭博.HS-SPME-GC-MS 分析温郁金不同炮制品的挥发性成分[J]. 中国实验方剂学杂志,2019,25(24):136
MA YY,LU JQ,PENG B.Analysis of volatile components of different processed Products of Curcuma wenyujin Radix by HS-SPME-GC-MS[J]. Chin J Exp Trap Med Form,2019,25(24):136
[138] CAMPILLO N,GAVAZOV K,VIñAS P ,et al.Liquid-phase microextraction:update May 2016 to December 2018[J]. Taylor & Francis,2020,55(4)
[139] LI L,HUANG M,SHAO J,et al.Rapid determination of alkaloids in Macleaya cordata using ionic liquid extraction followed by multiple reaction monitoring UPLC-MS/MS analysis[J]. J Pharm Biomed Anal,2017,135(Complete):61
[140] 于秀培,冯芳,滕宝祺,等.分散液液微萃取-HPLC 法测定藿香正气口服液中厚朴酚与和厚朴酚含量[J]. 药学与临床研究, 2012,20(3):264
YU XP,FENG F,TENG BQ,et al.Dispersive liquid-liquid microextraction-HPLC for the determination of magnolol and Honokiol in Huoxiangzhengqi oral solution[J]. Pharm Clin Res, 2012,20(3):264
[141] ZHANG Y,CHEN X,LI J,et al.Salt-assisted dispersive liquid-liquid microextraction for enhancing the concentration of matrine alkaloids in traditional Chinese medicine and its preparations[J]. J Sep Sci,2018,41(18):3503.
[142] 周生葆,宋亚会,刘桂香,等.分散液液微萃取-高效液相色谱法测定枸杞中拟除虫菊酯类农药残留研究[J]. 现代农业科技, 2020(9):104
ZHOU SB,SONG YH,LIU GX,et al.Determination of pyrethroid pesticide residues inLycium barbarumby dispersive liquid-liquid microextraction and high performance liquid chromatography[J]. Mod Agric Sci Technd,2020(9):104,109
[143] AKHTAR I,JAVAD S,ANSARI M,et al.Process optimization for microwave assisted extraction ofFoeniculum vulgareMill. using response surface methodology[J]. J King Saud Univ Sci,2020, 32(2):1451
[144] AKBARI S,ABDURAHMAN NH,YUNUS RM.Optimization of saponins,phenolics,and antioxidants extracted from fenugreek seeds using microwave-assisted extraction and response surface methodology as an optimizing tool[J]. Compt Rend Chim,2019, 22(11):714
[145] TSALTAKI C,KATSOULI M,KEKES T,et al.Comparison study for the recovery of bioactive compounds from Tribulus terrestris, Panax ginseng,Gingko biloba,Lepidium meyenii,Turnera diffusaandWithania somniferaby using microwave-assisted,ultrasound-assisted and conventional extraction methods[J]. Ind Crop Prod, 2019,142:111875
[146] WEI E,YANG R,ZHAO H,et al.Microwave-assisted extraction releases the antioxidant polysaccharides from seabuckthorn (Hippophae rhamnoides L.) berries[J]. Int J Bio/Mac romd,2019, 123:280
[147] LU X,ZHENG Z,LI H,et al.Optimization of ultrasonic-microwave assisted extraction of oligosaccharides from lotus (Nelumbo nucifera Gaertn.) seeds[J]. Ind Crop Prod,2017,107:546
[148] KAUR P,KUMAR PD,GUPTA RC,et al.Simultaneous microwave assisted extraction and HPTLC quantification of mangiferin, amarogentin,and swertiamarin in Swertia species from Western Himalayas[J].Ind Crop Prod,2019,132:449
[149] LEE SH,KIM JH.Kinetic and thermodynamic characteristics of microwave-assisted extraction for the recovery of paclitaxel from Taxus chinensis[J].Process Biochem,2019,76:187
[150] XIE JJ,LU J,QIAN ZM,et al.Optimization and comparison of five methods for extraction of coniferyl ferulate from Angelica sinensis[J].Molecules,2009,14(1):555
[151] LI W,WANG Z,WANG YP,et al.Pressurised liquid extraction combining LC-DAD-ESI/MS analysis as an alternative method to extract three major flavones in Citrus reticulata ‘Chachi’ (Guangchenpi)[J].Food Chem,2012,130(4):1044
[152] SHEN Y,HAN C,JIANG Y,et al.Rapid quantification of four major bioactive alkaloids in Corydalis decumbens (Thunb.) Pers.by pressurised liquid extraction combined with liquid chromatography-triple quadrupole linear ion trap mass spectrometry[J].Talanta,2011,84(4):1026
[153] YI Y,ZHANG QW,LI SL,et al.Simultaneous quantification of major flavonoids in“ Bawanghua”,the edible flower of Hylocereus undatus using pressurised liquid extraction and high performance liquid chromatography[J].Food Chem,2012,135(2):528
[154] ÇAM M,HIŞIL Y.Pressurised water extraction of polyphenols from pomegranate peels[J].Food Chem,2010,123(3):878
[155] MATSHEDISO PG,CUKROWSKA E,CHIMUKA L.Development of pressurised hot water extraction (PHWE) for essential compounds from Moringa oleifera leaf extracts[J].Food Chem,2015,172:423
[156] Sarafraz-Yazdi A,Razavi N.Application of molecularly-imprinted polymers in solid-phase microextraction techniques[J].TrAC Trends Anal Chem,2015,73:81
[157] RAHIMI M,BAHAR S,HEYDARI R,et al.Determination of quercetin using a molecularly imprinted polymer as solid-phase microextraction sorbent and high-performance liquid chromatography[J].Microchem J,2019,148:433
[158] 朱智博,麻清琳,梁爱珍,等.分子印迹- 基质固相分散技术分离分析矮地茶中岩白菜素[J].分析试验室,2013,32(11):108
ZHU ZB,MA QL,LIANG AZ,et al.Determination of bergenin in Ardisia japonica by molecularly imprinted-matrix Solid phase dispersion extraction[J].Chin J Anal Lab,2013,32(11):108
[159] HONG Y,CHEN L.Extraction of anthraquinones from rhubarb by a molecularly imprinted-matrix solid-phase dispersion method with HPLC detection[J].Anal Lett,2013,46(14):2235
[160] WANG Z,SUN R,WANG Y,et al.Determination of phenolic acids and flavonoids in raw propolis by silica-supported ionic liquid-based matrix solid phase dispersion extraction high performance liquid chromatography-diode array detection[J].J Chromatogr B, 2014,969:205
