快速分析

牛黄类药材及牛胆的红外光谱特征性分析与研究

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  • 中国食品药品检定研究院,北京 102629
第一作者 Tel:(010)53851576;E-mail:xiongjing@nifdc.org.cn
* Tel:(010)53852081;E-mail:san0373@163.com

修回日期: 2020-09-03

  网络出版日期: 2024-07-15

Analysis and research of succession medicinal substances of cow-bezoar and cattle bile with infrared spectroscopy

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  • National Institutes for Food and Drug Control,Beijing 102629,China

Revised date: 2020-09-03

  Online published: 2024-07-15

摘要

目的:对牛黄类药材及牛胆的红外光谱进行特征性分析和研究。方法:使用溴化钾压片法对样品进行红外光谱测定,以溴化钾作空白,每批样品扫描32 次,分辨率设为4 cm-1,扫描范围为4 000~400 cm-1结果:牛黄类药材及牛胆粉在3 400、1 725、1 650、1 555、1 450、1 250、1 218、1 046 和1 000~900 cm-1的波数范围具有一定的特征性。结论:红外光谱可快速表征牛黄类药材的特征,在牛黄类药材的特征性研究中具有较好的应用。

本文引用格式

熊婧, 何兰, 魏锋, 马双成, 石岩 . 牛黄类药材及牛胆的红外光谱特征性分析与研究[J]. 药物分析杂志, 2021 , 41(4) : 735 -740 . DOI: 10.16155/j.0254-1793.2021.04.23

Abstract

Objective: To study and analyze succession medicinal substances of cow-bezoar and cattle bile with infrared spectroscopy. Methods: The infrared spectrum determination was performed by potassium bromide pellet technique with potassium bromide used as blank and 4 cm-1 set as resolution,in the wave-number range of 4 000-400 cm-1. Results: The peaks at 3 400 cm-1,1 725 cm-1,1 650 cm-1,1 555 cm-1,1 450 cm-1,1 250 cm-1, 1 218 cm-1,1 046 cm-1 and 1 000-900 cm-1 indicated differences among these succession medicinal substances of cow-bezoar and cattle bile. Conclusion: Infrared spectrum can quickly characterize the characteristics of succession medicinal substances of cow-bezoar,and can be applyed in the characteristics study of these medicines.

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